N,N,N',N'-tetramethyl-N''-[3-(trimethoxysilyl)propyl]guanidine synthesis
1synthesis methods
- Product Name:N,N,N',N'-tetramethyl-N''-[3-(trimethoxysilyl)propyl]guanidine
- CAS Number:69709-01-9
- Molecular formula:C11H27N3O3Si
- Molecular Weight:277.44
Yield: 18%
Reaction Conditions:
Stage #1:N,N,N',N'-tetramethylguanidine in 5,5-dimethyl-1,3-cyclohexadiene at 120; for 2 h;Inert atmosphere;
Stage #2:3-Chloropropyltrimethoxysilan in 5,5-dimethyl-1,3-cyclohexadiene at 120; for 9 h;Inert atmosphere;
References:
Yang, Hengquan;Ma, Zhancheng;Qing, Yong;Xie, Guangyong;Gao, Jie;zhang, Li;Gao, Jinhua;du, Lin [Applied Catalysis A: General,2010,vol. 382,# 2,p. 312 - 321] Location in patent:experimental part