7-BROMO-1,2,3,4-TETRAHYDROCYCLOPENTA[B]INDOLE synthesis
- Product Name:7-BROMO-1,2,3,4-TETRAHYDROCYCLOPENTA[B]INDOLE
- CAS Number:164736-47-4
- Molecular formula:C11H10BrN
- Molecular Weight:236.11
622-88-8
313 suppliers
$8.00/5g
120-92-3
425 suppliers
$11.00/25g
164736-47-4
34 suppliers
$68.50/250mg
Yield: 92.3%
Reaction Conditions:
in ethanol for 10 h;Reflux;
Steps:
1.1-3
116.2 g (0.520 mol) of synthesized in [Scheme 2], 43.7 g (0.520 mol) of cyclopentanone and 1162.0 ml of ethanol were added to a 2 L round bottom flask and refluxed for 10 hours. After the reaction was completed, the reaction solution was concentrated and then column chromatography was used to obtain 120.0 g (yield 92.3%) of <1-c> .
References:
SFC Ltd.;Kim Si-in;Kim Nam-i KR102004387, 2019, B1 Location in patent:Paragraph 0279; 0292-0297
106-40-1
491 suppliers
$12.00/5g
164736-47-4
34 suppliers
$68.50/250mg
59-88-1
374 suppliers
$15.00/10g
164736-47-4
34 suppliers
$68.50/250mg