7-Iodo-7-deaza-D-guanosine synthesis
- Product Name:7-Iodo-7-deaza-D-guanosine
- CAS Number:444020-71-7
- Molecular formula:C11H13IN4O5
- Molecular Weight:408.15
480439-92-7
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Yield:444020-71-7 91%
Reaction Conditions:
with sodium hydroxide for 5 h;Reflux;
Steps:
2.4 synthesis of 7-deaza-7-iodoguanosine
Compound GD (506mg, 1.20mmol) disposed 25mL sodium hydroxide solution (2N) was refluxed 5H, cooled and added to a solution of acetic acid, filtered, washed with a small amount of water, and dried to give a white solid 445mg i.e. the GI, a yield of 91%.
References:
CN103819523,2016,B Location in patent:Paragraph 0066; 0077; 0078; 0079
873792-94-0
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873792-67-7
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149765-16-2
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$63.00/100mg
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7355-55-7
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$14.00/250mg
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