(7-methyl-1H-indol-3-yl)acetonitrile synthesis
- Product Name:(7-methyl-1H-indol-3-yl)acetonitrile
- CAS Number:858232-97-0
- Molecular formula:C11H10N2
- Molecular Weight:170.21
Yield:858232-97-0 72%
Reaction Conditions:
Stage #1: 2-aminoacetonitrile hydrochloridewith sodium nitrite in water at 55;
Stage #2: 7-methyl-1H-indolewith meso-tetraphenylporphyrin iron(III) chloride in dichloromethane;water at 20; for 2.33 h;Inert atmosphere;
References:
Hock, Katharina J.;Knorrscheidt, Anja;Hommelsheim, Renè;Ho, Junming;Weissenborn, Martin J.;Koenigs, Rene M. [Angewandte Chemie - International Edition,2019,vol. 58,# 11,p. 3630 - 3634][Angew. Chem.,2019,vol. 131,# 11,p. 3669 - 3673,5] Location in patent:supporting information
13712-78-2
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858232-97-0
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