Phenanthro(1,2-c)furan-1(3H)-one, 3b,4,5,9b,10,11-hexahydro-6-methoxy- 9b-methyl-7-(1-methylethyl)-, (3bR-trans)- synthesis

6synthesis methods

Product Name:Phenanthro(1,2-c)furan-1(3H)-one, 3b,4,5,9b,10,11-hexahydro-6-methoxy- 9b-methyl-7-(1-methylethyl)-, (3bR-trans)-
CAS Number:74311-48-1
Molecular formula:C21H26O3
Molecular Weight:326.43

201230-82-2 Synthesis

Yield:74311-48-1 93%

Reaction Conditions:

with tributyl-amine;lithium chloride;tetrakis(triphenylphosphine) palladium⁽⁰⁾ in acetonitrile at 65; under 760.051 Torr;Carbonylation;cyclization;

References:

Yang, Dan;Ye, Xiang-Yang;Xu, Ming [Journal of Organic Chemistry,2000,vol. 65,# 7,p. 2208 - 2217]

201230-82-2 Synthesis

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