ChemicalBook CAS DataBase List 3-Azido-1,2-di-O-acetyl-5-O-(4-methylbenzoyl)-3-deoxy-beta-D-ribofuranose

3-Azido-1,2-di-O-acetyl-5-O-(4-methylbenzoyl)-3-deoxy-beta-D-ribofuranose synthesis

5synthesis methods

Product Name:3-Azido-1,2-di-O-acetyl-5-O-(4-methylbenzoyl)-3-deoxy-beta-D-ribofuranose
CAS Number:75096-64-9
Molecular formula:C17H19N3O7
Molecular Weight:377.3487

75096-60-5 Synthesis

1,2-O-Isopropylidene-5-O-(4-Methylbenzoyl)-alpha-D-xylofuranose

75096-60-5
25 suppliers
$50.00/250mg

3-Azido-1,2-di-O-acetyl-5-O-(4-methylbenzoyl)-3-deoxy-beta-D-ribofuranose

75096-64-9
4 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 93 percent / pyridine / 1,2-dichloro-ethane / 0.5 h / -10 °C
2: 51 percent / NaN₃ / ethanol / 5 h / Heating
3: 1.) formic acid, 2.) pyridine / 1.) 50 deg C, 1 h, 2.) room temp. 2 h

References:

Ozols, Ainars M.;Azhayev, Alexy V.;Dyatkina, Natalia B.;Krayevsky, Alexander A. [Synthesis,1980,# 7,p. 557 - 559]