2-(3,4-DICHLORO-PHENYL)-5-METHYL-2H-PYRAZOL-3-YLAMINE synthesis
1synthesis methods
- Product Name:2-(3,4-DICHLORO-PHENYL)-5-METHYL-2H-PYRAZOL-3-YLAMINE
- CAS Number:76606-68-3
- Molecular formula:C10H9Cl2N3
- Molecular Weight:242.1
Yield:-
Steps:
5-Amino-3-methyl-1-(3,4-dichlorophenyl) pyrazole
5-Amino-3-methyl-1-(3,4-dichlorophenyl) pyrazole 3,4-Dichlorophenyl hydrazine HCl (50.0 g.) was reacted with 3-amino-2-butene nitrile (18.31 g.) as described in Example XLIII to give 18.7 g. product, mp 110°-112°. Analyzed for C10 H9 Cl2 N3; Theoretical; C=49.61, H=3.74, N=17.35 Found; C=50.09, H=3.75, N=17.43
References:
US4226773,1980,A