1H-Pyrrole-2-carboxylicacid,3-hydroxy-,methylester(9CI) synthesis
- Product Name:1H-Pyrrole-2-carboxylicacid,3-hydroxy-,methylester(9CI)
- CAS Number:79068-31-8
- Molecular formula:C6H7NO3
- Molecular Weight:141.12
Yield:-
Reaction Conditions:
with sodium
Steps:
102 Methyl 3-hydroxy-1H-pyrrole-2-carboxylate
EXAMPLE 102 Methyl 3-hydroxy-1H-pyrrole-2-carboxylate Prepared by the method described in Example 101 from methyl glycinate (22 g, 0.25 moles), methyl α-chloroacrylate (29.8 g, 0.25 moles), and sodium (17 g, 0.74 moles). The following filtration through silica gel and evaporation of the filtrate, the product is obtained pure and crystalline (18.6 g); mp 100°-102° C.
References:
Warner-Lambert Company US4748183, 1988, A
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