2-AMino-6-broMo-2-(2-chlorophenyl)cyclohexanone-d4 HydrobroMide synthesis

4synthesis methods

Product Name:2-AMino-6-broMo-2-(2-chlorophenyl)cyclohexanone-d4 HydrobroMide
CAS Number:79499-60-8
Molecular formula:C12H10Br2ClD4NO
Molecular Weight:387.5313

6740-86-9 Synthesis

1-bromocyclopentyl-o-chlorophenyl ketone

6740-86-9
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2-AMino-6-broMo-2-(2-chlorophenyl)cyclohexanone-d4 HydrobroMide

79499-60-8
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1) liq. NH₃, 2) HCl / 1) 4 h, 2) i-PrOH
2: 88 percent / various solvent(s) / 0.12 h / 180 °C
3: 82 percent / 48percent aq. HBr, Br₂ / 0.17 h / 70 °C

References:

Parcell, Robert F.;Sanchez, Joseph P. [Journal of Organic Chemistry,1981,vol. 46,# 25,p. 5055 - 5060]

2-AMINO-2-(2-CHLOROPHENYL)CYCLOHEXANONE HYDROCHLORIDE

35211-10-0
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79499-60-8
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References

1-[(2-Chlorophenyl)(imino)methyl]cyclopentanol Hydrochloride

79499-58-4
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79499-60-8
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References

Cyclopentanol, 1-[(2-chlorophenyl)iminomethyl]-

79499-57-3
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79499-60-8
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References