8-Nitro-1,4-Dioxaspiro[4.5]Decane synthesis
- Product Name:8-Nitro-1,4-Dioxaspiro[4.5]Decane
- CAS Number:635728-10-8
- Molecular formula:C8H13NO4
- Molecular Weight:187.19
3638-64-0
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38053-91-7
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107-21-1
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635728-10-8
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Yield:635728-10-8 51%
Reaction Conditions:
Stage #1: 1-nitroethylene;2-trimethylsilyloxy-1,3-butadiene in benzene;Heating;
Stage #2: ethylene glycolwith toluene-4-sulfonic acid in benzene;Heating;
References:
Bonjoch, Josep;Diaba, Fa?za;Puigbó, Gemma;Peidró, Emma;Solé, Daniel [Tetrahedron Letters,2003,vol. 44,# 46,p. 8387 - 8390]