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ChemicalBook CAS DataBase List Phosphine, (2,2-dimethyl-1,3-propanediyl)bis[diphenyl-
80326-98-3

Phosphine, (2,2-dimethyl-1,3-propanediyl)bis[diphenyl- synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: dmap; pyridine / dichloromethane / 4 h / 0 °C / Inert atmosphere; Schlenk technique
2.1: n-butyllithium / tetrahydrofuran / 1 h / 0 - 25 °C / Inert atmosphere; Schlenk technique
2.2: 4 h / 25 °C / Inert atmosphere; Schlenk technique

References:

O'Neill, Matthew J.;Riesebeck, Tim;Cornella, Josep [Angewandte Chemie - International Edition,2018,vol. 57,# 29,p. 9103 - 9107][Angew. Chem.,2018,vol. 130,p. 9241 - 9245,5]