1H-Indole-2-carboxaldehyde, 4,5,6,7-tetrahydro- (9CI) synthesis
- Product Name:1H-Indole-2-carboxaldehyde, 4,5,6,7-tetrahydro- (9CI)
- CAS Number:80744-01-0
- Molecular formula:C9H11NO
- Molecular Weight:149.19
108-94-1
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80744-01-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: hydroxylamine hydrochloride; potassium hydroxide / dimethyl sulfoxide / 0.5 h / 70 °C
1.2: 4 h / 120 °C
2.1: trichlorophosphate / 0.25 h / 20 - 25 °C
2.2: 0.25 h / 0 - 85 °C
References:
Stark, Daniel G.;Williamson, Patrick;Gayner, Emma R.;Musolino, Stefania F.;Kerr, Ryan W. F.;Taylor, James E.;Slawin, Alexandra M. Z.;O'Riordan, Timothy J. C.;Macgregor, Stuart A.;Smith, Andrew D. [Organic and Biomolecular Chemistry,2016,vol. 14,# 38,p. 8957 - 8965]
100-64-1
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80744-01-0
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13754-86-4
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80744-01-0
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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80744-01-0
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1000210-73-0
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80744-01-0
36 suppliers
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