ChemicalBook CAS DataBase List (Z)-2-((3S,5R)-3,5-bis((tert-butyldiMethylsilyl)oxy)-2-Methylenecyclohexylidene)ethanol

(Z)-2-((3S,5R)-3,5-bis((tert-butyldiMethylsilyl)oxy)-2-Methylenecyclohexylidene)ethanol synthesis

12synthesis methods

Product Name:(Z)-2-((3S,5R)-3,5-bis((tert-butyldiMethylsilyl)oxy)-2-Methylenecyclohexylidene)ethanol
CAS Number:81506-24-3
Molecular formula:C21H42O3Si2
Molecular Weight:398.73

129482-80-0
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(Z)-2-((3S,5R)-3,5-bis((tert-butyldiMethylsilyl)oxy)-2-Methylenecyclohexylidene)ethanol

81506-24-3
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Yield:81506-24-3 97%

Reaction Conditions:

with diisobutylaluminium hydride in toluene;

References:

Mourino, Antonio;Torneiro, Mercedes;Vitale, Cristian;Fernandez, Sara;Perez-Sestelo, Jose;Anne, Sofia;Gregorio, Carlos [Tetrahedron Letters,1997,vol. 38,# 26,p. 4713 - 4716]

Acetic acid, 2-[(3S,5R)-3,5-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-methylenecyclohexylidene]-, ethyl ester, (2Z)-

81570-20-9
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81506-24-3
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References

Methanesulfonic acid, 1,1,1-trifluoro-, (1Z,3S,5S)-3,5-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-1-(2-hydroxyethylidene)-6-hepten-1-yl ester

342645-98-1
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81506-24-3
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227961-42-4 Synthesis

(E)-2-((3S,5R)-3,5-bis((tert-butyldimethylsilyl)oxy)-2-methylenecyclohexylidene)ethan-1-ol

227961-42-4
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References

Acetic acid, 2-[(3S,5R)-3,5-bis[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-methylenecyclohexylidene]-, ethyl ester, (2E)-

81506-23-2
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81506-24-3
29 suppliers
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References

39903-97-4
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81506-24-3
29 suppliers
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References