BENZAMIDE, N-[(1-ETHYL-2-PYRROLIDINYL)METHYL]-2-HYDROXY-3-IODO-6-METHOXY- synthesis
- Product Name:BENZAMIDE, N-[(1-ETHYL-2-PYRROLIDINYL)METHYL]-2-HYDROXY-3-IODO-6-METHOXY-
- CAS Number:84226-06-2
- Molecular formula:C15H21IN2O3
- Molecular Weight:404.24
Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.1 h / 20 °C
1.2: 24 h / 20 °C
2.1: tetrafluoroboric acid / ethanol; water / 0.5 h / 20 °C
2.2: 0.7 h / 36 °C
References:
Racys, Daugirdas T.;Warrilow, Catherine E.;Pimlott, Sally L.;Sutherland, Andrew [Organic Letters,2015,vol. 17,# 19,p. 4782 - 4785]
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