ethyl 5-hydroxy-2,2-dimethyl-3-oxopentanoate(SALTDATA: FREE) synthesis

3synthesis methods

Product Name:ethyl 5-hydroxy-2,2-dimethyl-3-oxopentanoate(SALTDATA: FREE)
CAS Number:84752-35-2
Molecular formula:C9H16O4
Molecular Weight:188.22

600-00-0 Synthesis

600-00-0
263 suppliers
$13.00/5g

109-78-4 Synthesis

109-78-4
349 suppliers
$10.00/1g

ethyl 5-hydroxy-2,2-dimethyl-3-oxopentanoate(SALTDATA: FREE)

84752-35-2
9 suppliers
$70.00/1g

Yield:84752-35-2 71%

Reaction Conditions:

Stage #1: ethyl 2-bromoisobutyrate;3-Hydroxypropionitrilewith zinc in tetrahydrofuran;Reformatsky-type reaction;
Stage #2: with hydrogenchloride in tetrahydrofuran;

References:

Fuerstner;Mathes;Grela [Chemical Communications,2001,# 12,p. 1057 - 1059]

4-Pentenoic acid, 5-hydroxy-2,2-dimethyl-3-oxo-, ethyl ester

84752-50-1
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inquiry

84752-35-2
9 suppliers
$70.00/1g

References

2,2-DIMETHYL-ACETOACETIC ACID ETHYL ESTER

597-04-6
40 suppliers
$70.00/100mg

84752-35-2
9 suppliers
$70.00/1g

References