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ChemicalBook CAS DataBase List Benzyl 2-(AcetylaMino)-2-deoxy-3-O-[3,4,6-tri-O-acetyl-2-deoxy-2-phthaliMido-β-D-glucopyranosyl]-α-D-galactopyranoside
85069-37-0

Benzyl 2-(AcetylaMino)-2-deoxy-3-O-[3,4,6-tri-O-acetyl-2-deoxy-2-phthaliMido-β-D-glucopyranosyl]-α-D-galactopyranoside synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) silver trifluoromethanesulfonate, 2,4,6-trimethylpyridine, molecular sieves type 4A / 1.) dichloromethane, r.t., 1 h; 2.) dichloromethane, 4 h
2: 89.9 percent / 60 percent acetic acid / H2O / 1.5 h / 85 °C

References:

Abbas;Barlow;Matta [Carbohydrate research,1983,vol. 112,# 2,p. 201 - 211]