ETHYL 4-(2-HYDROXY-5-METHYL-3-NITROPHENYL)-2,4-DIOXOBUTANOATE synthesis

2synthesis methods

Product Name:ETHYL 4-(2-HYDROXY-5-METHYL-3-NITROPHENYL)-2,4-DIOXOBUTANOATE
CAS Number:859843-60-0
Molecular formula:C13H13NO7
Molecular Weight:295.24

2'-HYDROXY-5'-METHYL-3'-NITROACETOPHENONE

66108-30-3
80 suppliers
$20.00/1g

95-92-1 Synthesis

95-92-1
431 suppliers
$5.00/5G

ETHYL 4-(2-HYDROXY-5-METHYL-3-NITROPHENYL)-2,4-DIOXOBUTANOATE

859843-60-0
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Yield:859843-60-0 86%

Reaction Conditions:

Stage #1: 2-hydroxy-5-methyl-3-nitroacetophenonewith sodium ethanolate in ethanol; for 0.5 h;
Stage #2: oxalic acid diethyl ester in ethanol; for 2 h;Heating;Claisen condensation;

References:

Anderluh, Marko;Marc, Gasper;Dolenc, Marija Sollner [Synthetic Communications,2005,vol. 35,# 11,p. 1461 - 1470]

1450-72-2 Synthesis

1450-72-2
200 suppliers
$6.00/1g

859843-60-0
18 suppliers
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References

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