Methyl 2-methoxy-5-methyl-3-nitrobenzenecarboxylate synthesis
- Product Name:Methyl 2-methoxy-5-methyl-3-nitrobenzenecarboxylate
- CAS Number:863226-26-0
- Molecular formula:C10H11NO5
- Molecular Weight:225.2
89-56-5
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 95 percent / sulfuric acid / 24 h / Heating
2: 72 percent / nitric acid / H2O / 24 h / 20 °C
3: 80 percent / potassum carbonate; 18-crown-6 / acetone / 36 h / 20 °C
References:
Yi, Hui-Ping;Li, Chuang;Hou, Jun-Li;Jiang, Xi-Kui;Li, Zhan-Ting [Tetrahedron,2005,vol. 61,# 33,p. 7974 - 7980]
22717-57-3
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