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873072-60-7

3-Methyl-1H-thieno[2,3-c]pyrazole-5-carboxylic acid synthesis

3synthesis methods
1H-Thieno[2,3-c]pyrazole-5-carboxylic acid, 1-[(4-methoxyphenyl)methyl]-3-methyl-

873072-58-3
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3-Methyl-1H-thieno[2,3-c]pyrazole-5-carboxylic acid

873072-60-7
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Yield:873072-60-7 59%

Reaction Conditions:

with trifluoroacetic acid in dichloromethane at 120; for 0.333333 h;microwave irradiation;

References:

Akritopoulou-Zanze, Irini;Darczak, Daria;Sarris, Kathy;Phelan, Kathleen M.;Huth, Jeffrey R.;Song, Danying;Johnson, Eric F.;Jia, Yong;Djuric, Stevan W. [Bioorganic and Medicinal Chemistry Letters,2006,vol. 16,# 1,p. 96 - 99]