1-[4-[[[(1,1-DiMethylethyl)diMethylsilyl]oxy]Methyl]phenyl]-2,2,2-trifluoro-ethanone synthesis
- Product Name:1-[4-[[[(1,1-DiMethylethyl)diMethylsilyl]oxy]Methyl]phenyl]-2,2,2-trifluoro-ethanone
- CAS Number:87736-75-2
- Molecular formula:C15H21F3O2Si
- Molecular Weight:318.41
383-63-1
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![tert-butyl[(4-iodophenyl)methoxy]dimethylsilane](/CAS/20200401/GIF/147283-96-3.gif)
147283-96-3
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87736-75-2
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Yield:87736-75-2 99%
Reaction Conditions:
Stage #1: 4-(tert-butyldimethylsiloxymethyl)iodobenzenewith n-butyllithium in tetrahydrofuran;hexane at -78; for 0.75 h;
Stage #2: ethyl trifluoroacetate, in tetrahydrofuran;hexane at -78; for 1.25 h;
References:
Nakamoto, Kosuke;Ueno, Yoshihito [Journal of Organic Chemistry,2014,vol. 79,# 6,p. 2463 - 2472]
360-92-9
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$23.39/1g
87736-74-1
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$650.00/100mg
87736-75-2
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$155.00/50mg
383-63-1
503 suppliers
$10.00/25g
87736-74-1
64 suppliers
$650.00/100mg
87736-75-2
26 suppliers
$155.00/50mg
340-07-8
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$6.00/1g
87736-74-1
64 suppliers
$650.00/100mg
87736-75-2
26 suppliers
$155.00/50mg
873-75-6
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$6.00/5g
87736-75-2
26 suppliers
$155.00/50mg