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((Butylsulfinyl)(phenyl)methyl)diphenylphosphine oxide synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1) TMEDA, n-BuLi / 1) THF, RT, 15 min; 2) RT, 15 min
3: 2) NH4Cl / 1) THF, -78 deg C, 1 h; 2) H2O

References:

Porskamp, Pascal A. T. W.;Lammerink, Ben H. M.;Zwanenburg, Binne [Journal of Organic Chemistry,1984,vol. 49,# 2,p. 263 - 268]