(5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)MethanaMine hydrochloride synthesis
- Product Name:(5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-yl)MethanaMine hydrochloride
- CAS Number:880495-82-9
- Molecular formula:C12H19BN2O2
- Molecular Weight:234.1
31181-90-5
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 100 percent / I2; aq. NH3 / tetrahydrofuran / 4 h / 20 °C
2: 64 percent / PdCl2(dppf); KOAc / dimethylsulfoxide / 25 h / 80 °C
3: 100 percent / H2; acetic acid / Pd/C / 16 h / 20 °C
References:
Wiles, Jason A.;Song, Yongsheng;Wang, Qiuping;Lucien, Edlaine;Hashimoto, Akihiro;Cheng, Jijun;Marlor, Christopher W.;Ou, Yangsi;Podos, Steven D.;Thanassi, Jane A.;Thoma, Christy L.;Deshpande, Milind;Pucci, Michael J.;Bradbury, Barton J. [Bioorganic and Medicinal Chemistry Letters,2006,vol. 16,# 5,p. 1277 - 1281]
741709-63-7
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97483-77-7
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