(2S,3S)-2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-3-methylpentane(thioperoxoic) OS-acid synthesis
- Product Name:(2S,3S)-2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)-3-methylpentane(thioperoxoic) OS-acid
- CAS Number:881913-47-9
- Molecular formula:C21H23NO3S
- Molecular Weight:369.48
71989-23-6
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881913-47-9
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Yield:881913-47-9 88%
Reaction Conditions:
with sodium sulfide;1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in N,N-dimethyl-formamide; for 3 h;Inert atmosphere;
References:
Vishwanatha;Samarasimhareddy;Sureshbabu, Vommina V. [Synlett,2012,# 1,art. no. D20211ST,p. 89 - 92] Location in patent:experimental part
![L-Isoleucine, N-[(9H-fluoren-9-ylmethoxy)carbonyl]-, anhydride with 2-methylpropyl hydrogen carbonate (9CI)](/CAS/20211123/GIF/98807-43-3.gif)
98807-43-3
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881913-47-9
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