9 10-BIS(TMEDA)ANTHRACENE BISZINC synthesis
- Product Name:9 10-BIS(TMEDA)ANTHRACENE BISZINC
- CAS Number:106682-14-8
- Molecular formula:C26H38N4.2Cl2Zn
- Molecular Weight:679.206
106712-13-4
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Yield: 87%
Reaction Conditions:
in methanoladdn. of ligand soln. to a hot stirred soln. of ZnCl2; cooled slowly to room temp., crystn., filtered, washed (MeOH), dried at 70°C in vac. overnight, elem. anal.;
References:
Nanjappan, Palaniappan;Czarnik, Anthony W. [Journal of the American Chemical Society,1987,vol. 109,# 6,p. 1826 - 1833]