9-AMino(9-deoxy)epi-diquinidine trihydrochloride synthesis
- Product Name:9-AMino(9-deoxy)epi-diquinidine trihydrochloride
- CAS Number:522600-31-3
- Molecular formula:C20H27N3O
- Molecular Weight:325.45
1435-55-8
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Yield: 87%
Reaction Conditions:
Stage #1:hydroquinidine with di-isopropyl azodicarboxylate;diphenyl phosphoryl azide;triphenylphosphine in tetrahydrofuran at 0 - 50; for 16 h;
Stage #2: with water in tetrahydrofuran at 20; for 3 h;
References:
Oliva, Cristina G.;Silva, Artur M. S.;Resende, Diana I. S. P.;Paz, Filipe A. A.;Cavaleiro, Jose A. S. [European Journal of Organic Chemistry,2010,# 18,p. 3449 - 3458] Location in patent:experimental part
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