9-(BroMoMethyl)nonadecane synthesis
- Product Name:9-(BroMoMethyl)nonadecane
- CAS Number:69620-20-8
- Molecular formula:C20H41Br
- Molecular Weight:361.44
112-29-8
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$6.00/25g
69620-20-8
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$33.00/25g
Yield:-
Steps:
Multi-step reaction with 5 steps
1.1: sodium methylate / N,N-dimethyl-formamide / 0.5 h / 80 °C / Large scale
1.2: 2 h / 120 °C / Large scale
2.1: sodium methylate / N,N-dimethyl-formamide / 0.5 h / 80 °C / Large scale
2.2: 2 h / 120 °C / Large scale
3.1: lithium chloride / N,N-dimethyl-formamide; water / 24 h / 160 °C / Large scale
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C / Cooling with ice
5.1: 1H-imidazole; triphenylphosphine; carbon tetrabromide / dichloromethane / 3 h / 20 °C / Cooling with ice
References:
CN108821937,2018,A
5333-42-6
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$30.00/10g
69620-20-8
80 suppliers
$33.00/25g