9-METHYL-6-THIOPURINE synthesis
- Product Name:9-METHYL-6-THIOPURINE
- CAS Number:1006-20-8
- Molecular formula:C6H6N4S
- Molecular Weight:166.2
2346-74-9
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Yield:1006-20-8 95%
Reaction Conditions:
with thiourea in ethanol at 100; for 3 h;
Steps:
1 Example 1:
Prepare a solution of compound 1b in EtOH,To a solution of compound 1b (338 mg, 2.0 mmol) in EtOH (10 mL) was added commercially available thiourea (228 mg, 3 mmol),The reaction was heated to 100°C with stirring and refluxing for 3 hours.After the TCL detection reaction was completed, suction filtration and washing the precipitate with anhydrous EtOH,Spin dry to give compound 2b, 317 mg (white solid), yield 95%.
References:
CN111333651,2020,A Location in patent:Paragraph 0033-0036
52602-68-3
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1006-20-8
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875-31-0
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$130.00/50mg
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