ChemicalBook CAS DataBase List 9-Methyl-9H-beta-carboline

9-Methyl-9H-beta-carboline synthesis

6synthesis methods

Product Name:9-Methyl-9H-beta-carboline
CAS Number:2521-07-5
Molecular formula:C12H10N2
Molecular Weight:182.22

9-Methyl-β-carboline may be prepared by performing the Eschweiler–Clarke reaction on freebase β-carboline (norharmane).

1H-Indole-2-carboxaldehyde, 3-iodo-1-methyl-

372954-67-1
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2521-07-5
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 100 percent / Et₃N; 1percent CuI / 2percent PdCl₂(PPh₃)2 / 16 h / 60 °C
2: 24 h / 100 °C
3: 41 percent / 10percent CuI / dimethylformamide / 92 h / 100 - 130 °C

References:

Zhang, Haiming;Larock, Richard C. [Journal of Organic Chemistry,2002,vol. 67,# 20,p. 7048 - 7056]

1H-PYRIDO[3,4-B]INDOLE, 2,3,4,9-TETRAHYDRO-9-METHYL-

16502-02-6
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$3230.00/5G

2521-07-5
113 suppliers
$19.00/100mg

References

1H-Indole, 1,2-dimethyl-3-[(1E)-2-nitroethenyl]-

122631-41-8
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2521-07-5
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References

1H-Indole-2-carboxaldehyde, 3-[2-(1-hydroxycyclohexyl)ethynyl]-1-methyl-

474267-09-9
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2521-07-5
113 suppliers
$19.00/100mg

References

62747-53-9
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2521-07-5
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$19.00/100mg

References

9-Methyl-9H-beta-carboline Related Search:

1-TRIFLUOROMETHYL-2,3,4,9-TETRAHYDRO-1H-B-CARBOLINE

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