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ChemicalBook CAS DataBase List 9-OXO-9H-FLUORENE-4-CARBOXAMIDE

9-OXO-9H-FLUORENE-4-CARBOXAMIDE synthesis

9synthesis methods
-

Yield:42135-38-6 87%

Reaction Conditions:

Stage #1: 9-oxo-9H-fluorene-4-carboxylic acidwith phosphorus pentachloride in 5,5-dimethyl-1,3-cyclohexadiene at 90 - 100; for 1 h;
Stage #2: with ammonium hydroxide

References:

Ghamari, Pegah;Hamzehpoor, Ehsan;Niazi, Muhammad Rizwan;Perepichka, Dmitrii F.;Perepichka, Igor F. [Chemical Communications,2020,vol. 56,# 47,p. 6432 - 6435] Location in patent:supporting information

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