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ChemicalBook CAS DataBase List (+)-(1R,2R,5R)--Ethyl [(2-Hydroxypinan-3-ylene)aMino]acetate

(+)-(1R,2R,5R)--Ethyl [(2-Hydroxypinan-3-ylene)aMino]acetate synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide; pyridine / water; acetone / 60 h / Reflux
2.1: ammonia / toluene / 1 h
2.2: 5 h / Dean-Stark; Reflux

References:

US2016/83335,2016,A1