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Structured search
18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
911227-46-8

5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE synthesis

4synthesis methods
2-Pyridinecarboxamide, N,N-diethyl-

7606-13-5
15 suppliers
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Bis(pinacolato)diboron

73183-34-3
593 suppliers
$6.00/5g

5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE

911227-46-8
34 suppliers
$254.00/500mg

-

Yield:911227-46-8 74%

Reaction Conditions:

Stage #1: bis(pinacol)diboranewith (1,5-cyclooctadiene)(methoxy)iridium(I) dimer;4,4'-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-2,2’-bipyridine in hexane at 60; for 0.5 h;Inert atmosphere;Glovebox;Sealed tube;
Stage #2: N,N-diethyl-2-pyridinecarboxamidewith bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum in hexane at 20; for 18 h;Sealed tube;

References:

Yang, Lichen;Semba, Kazuhiko;Nakao, Yoshiaki [Angewandte Chemie - International Edition,2017,vol. 56,# 17,p. 4853 - 4857][Angew. Chem.,2017,vol. 129,# 17,p. 4931 - 4935] Location in patent:supporting information

Bis(pinacolato)diboron

73183-34-3
593 suppliers
$6.00/5g

673485-54-6 Synthesis
5-BROMO-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE

673485-54-6
34 suppliers
inquiry

5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE

911227-46-8
34 suppliers
$254.00/500mg

References
673485-54-6 Synthesis
5-BROMO-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE

673485-54-6
34 suppliers
inquiry

5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE

911227-46-8
34 suppliers
$254.00/500mg

References
5-BROMOPYRIDINE-2-CARBONYL CHLORIDE

137178-88-2
70 suppliers
$34.00/1g

5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE

911227-46-8
34 suppliers
$254.00/500mg

References

5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDINE-2-CARBOXYLIC ACID DIETHYLAMIDE Related Search:

2-(CYCLOPROPYLMETHOXY)-5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PYRIDINE 4-[5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)-PYRIDIN-2-YL]-PIPERAZINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER TERT-BUTYL N-METHYL-N-[5-(4,4,5,5-TETRAMETHYL-[1,3,2]DIOXABOROLAN-2-YL)PYRIDIN-2-YL]CARBAMATE 6-(4-FLUOROPHENYL)PYRIDINE-3-BORONIC ACID PINACOL ESTER 1-METHYL-4-[5-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABORALAN-2-YL)PYRIDINE-2-YL]PIPERAZINE Methyl 5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)picolinate 2-METHYLSULFANYL-5-(4,4,5,5-TETRAMETHYL-[1,3,2]-DIOXABOROLAN-2-YL)PYRIDINE 2-FORMYLPYRIDINE-5-BORONIC ACID PINACOLATE 2-(N-Methylaminocarbonyl)-5-pyridineboronic acid pincol ester