3-Cyclohexene-1-carboxylic acid, 6-methyl-, (1R,6R)- synthesis

2synthesis methods

Product Name:3-Cyclohexene-1-carboxylic acid, 6-methyl-, (1R,6R)-
CAS Number:92344-71-3
Molecular formula:C8H12O2
Molecular Weight:140.18

3-Cyclohexene-1-carbonyl chloride, 6-methyl-, trans- (9CI)

92284-36-1
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3-Cyclohexene-1-carboxylic acid, 6-methyl-, (1R,6R)-

92344-71-3
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Yield:-

Steps:

Multi-step reaction with 5 steps
2: 1) LDA 2) HMPT / 1) THF, 0 deg C 2) 25 deg C, 16h
3: HCl / tetrahydrofuran / 6 h / Heating
4: 40 percent / LAH / tetrahydrofuran / 16 h / Heating
5: 71 percent / Jones reagent

References:

Sonnet, Philip E.;McGovern, Terrence P.;Cunningham, Roy T. [Journal of Organic Chemistry,1984,vol. 49,# 24,p. 4639 - 4643]

3-Cyclohexene-1-methanol, 6-methyl-, (1S-trans)- (9CI)

92344-78-0
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92344-71-3
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References

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