t-Butyl 3,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1h-pyrrolo[2,3-b]pyridine-1-carboxylate95% synthesis
- Product Name:t-Butyl 3,5-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1h-pyrrolo[2,3-b]pyridine-1-carboxylate95%
- CAS Number:942070-54-4
- Molecular formula:C24H36B2N2O6
- Molecular Weight:470.17
138343-77-8
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$45.00/10mg
73183-34-3
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942070-54-4
20 suppliers
$45.00/10mg
Yield:942070-54-4 92%
Reaction Conditions:
Stage #1: bis(pinacol)diboranewith (1,5-cyclooctadiene)(methoxy)iridium(I) dimer;4,4'-di-tert-butyl-2,2'-bipyridine in tert-butyl methyl ether;Inert atmosphere;
Stage #2: 1-(tert-butoxycarbonyl)-1H-pyrrolo<2,3-b>pyridine in tert-butyl methyl ether at 80; for 0.333333 h;Inert atmosphere;Microwave irradiation;
References:
Harrisson, Peter;Morris, James;Marder, Todd B.;Steel, Patrick G. [Organic Letters,2009,vol. 11,# 16,p. 3586 - 3589] Location in patent:supporting information; experimental part
138343-77-8
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$45.00/10mg
25015-63-8
224 suppliers
$22.39/5G
942070-54-4
20 suppliers
$45.00/10mg