2,6-Bis(tributylstannyl)dithieno[3,2-b:2',3'-d]thiophene synthesis
- Product Name:2,6-Bis(tributylstannyl)dithieno[3,2-b:2',3'-d]thiophene
- CAS Number:944257-56-1
- Molecular formula:C32H56S3Sn2
- Molecular Weight:774.4
![DITHIENO[2,3-B:2',3'-D]THIOPHENE](/CAS/GIF/3593-75-7.gif)
3593-75-7
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944257-56-1
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Yield:944257-56-1 91%
Reaction Conditions:
Stage #1: dithieno[3,2-b;2',3'-d]thiophenewith n-butyllithium in tetrahydrofuran at -78 - 20; for 1 h;
Stage #2: tributyltin chloride in tetrahydrofuran at -78; for 0.5 h;
References:
Liang, Aihui;Gao, Yao;Asadpour, Reza;Wei, Zitang;Finkenauer, Blake P.;Jin, Linrui;Yang, Jiaqi;Wang, Kang;Chen, Ke;Liao, Peilin;Zhu, Chenhui;Huang, Libai;Boudouris, Bryan W.;Alam, Muhammad Ashraf;Dou, Letian [Journal of the American Chemical Society,2021,vol. 143,# 37,p. 15215 - 15223] Location in patent:supporting information