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ChemicalBook CAS DataBase List 1,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)pyrene
950779-13-2

1,6-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane-2-yl)pyrene synthesis

4synthesis methods
-

Yield:950779-13-2 99%

Reaction Conditions:

with palladium (II) [1,1'-bis(diphenylphosphanyl)ferrocene] dichloride;anhydrous potassium acetate in dimethyl sulfoxide at 80; for 16 h;Schlenk technique;Inert atmosphere;Miyaura Borylation Reaction;

References:

Xu, Kun;Fu, Yubin;Zhou, Youjia;Hennersdorf, Felix;Machata, Peter;Vincon, Ilka;Weigand, Jan J.;Popov, Alexey A.;Berger, Reinhard;Feng, Xinliang [Angewandte Chemie - International Edition,2017,vol. 56,# 50,p. 15876 - 15881][Angew. Chem.,2017,vol. 129,p. 16092 - 16097,6] Location in patent:supporting information