3,6-Bis(2-methylpropyl)-2,5-pyrazinediol 1,4-dioxide synthesis

1synthesis methods

Product Name:3,6-Bis(2-methylpropyl)-2,5-pyrazinediol 1,4-dioxide
CAS Number:957-86-8
Molecular formula:C12H20N2O4
Molecular Weight:256.3

Pyrazine, 2,5-dichloro-3,6-bis(2-methylpropyl)-

19803-47-5
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3,6-Bis(2-methylpropyl)-2,5-pyrazinediol 1,4-dioxide

957-86-8
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 22 percent / K₂S₂O₈, conc. H₂SO₄ / 48 h / Ambient temperature
2: 89 percent / sodium methoxide; conc. HCl / dioxane / 4 h / 110 °C

References:

Ohta, Akihiro;Yamamoto, Fusako;Arimura, Yasuhiko;Watanabe, Tokuhiro [Journal of Heterocyclic Chemistry,1982,vol. 19,p. 781 - 784]

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