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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 1H-Inden-4-ol, octahydro-1-[(1R,2E,4S)-5-hydroxy-1,4,5-triMethyl-2-hexen-1-yl]-7a-Methyl-, (1R,3aR,4S,7aR)-
95716-67-9

1H-Inden-4-ol, octahydro-1-[(1R,2E,4S)-5-hydroxy-1,4,5-triMethyl-2-hexen-1-yl]-7a-Methyl-, (1R,3aR,4S,7aR)- synthesis

6synthesis methods
(2S)-2-((1R,3aR,7aR)-4-(tert-butyldiMethylsilyloxy)-7a-Methyloctahydro-1H-inden-1-yl)propanal

104651-47-0
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1H-Inden-4-ol, octahydro-1-[(1R,2E,4S)-5-hydroxy-1,4,5-triMethyl-2-hexen-1-yl]-7a-Methyl-, (1R,3aR,4S,7aR)-

95716-67-9
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-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 1.) t-BuLi / 1.) THF, pentane, -78 to 0 deg C, 1.5 h, 2.) THF, rt, 15 h
2: 1.) Et2Zn
3: 93 percent / p-toluenesulfonic acid, H2O / dioxane / Ambient temperature
4: 95 percent / 48percent aq. HF / acetonitrile / 2.5 h

References:

Wilson;Davey;Guazzaroni [Journal of Organic Chemistry,1992,vol. 57,# 7,p. 2007 - 2012]

924-50-5 Synthesis
Methyl 3-methyl-2-butenoate

924-50-5
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1H-Inden-4-ol, octahydro-1-[(1R,2E,4S)-5-hydroxy-1,4,5-triMethyl-2-hexen-1-yl]-7a-Methyl-, (1R,3aR,4S,7aR)-

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References
1H-Inden-4-ol, octahydro-7a-methyl-1-[1-methyl-2-(2,4,5,5-tetramethyl-3-isoxazolidinyl)ethyl]-, [1R-[1α[R*(3S*,4S*)],3aβ,4α,7aα]]- (9CI)

95716-65-7
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1H-Inden-4-ol, octahydro-1-[(1R,2E,4S)-5-hydroxy-1,4,5-triMethyl-2-hexen-1-yl]-7a-Methyl-, (1R,3aR,4S,7aR)-

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References
4-Isoxazolidinemethanol, 2,5,5-trimethyl-3-[2-(octahydro-4-hydroxy-7a-methyl-1H-inden-1-yl)propyl]-, [1R-[1α[R*(3S*,4R*)],3aβ,4α,7aα]]- (9CI)

95716-63-5
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1H-Inden-4-ol, octahydro-1-[(1R,2E,4S)-5-hydroxy-1,4,5-triMethyl-2-hexen-1-yl]-7a-Methyl-, (1R,3aR,4S,7aR)-

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References
Toluene-4-sulfonic acid 3S-[2R-(4S-hydroxy-7R-methyl-octahydro-inden-1R-yl)-propyl]-2,5,5-trimethyl-isoxazolidin-4R-ylmethyl ester

95716-64-6
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1H-Inden-4-ol, octahydro-1-[(1R,2E,4S)-5-hydroxy-1,4,5-triMethyl-2-hexen-1-yl]-7a-Methyl-, (1R,3aR,4S,7aR)-

95716-67-9
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References

1H-Inden-4-ol, octahydro-1-[(1R,2E,4S)-5-hydroxy-1,4,5-triMethyl-2-hexen-1-yl]-7a-Methyl-, (1R,3aR,4S,7aR)- Related Search:

(1R,3aR,7aR)-1-((2R,5S,E)-6-hydroxy-5,6-diMethylhept-3-en-2-yl)-7a-Methylhexahydro-1H-inden-4(2H)-one (1R,3aR,7aR)-1-((2R,5S,Z)-6-hydroxy-5,6-dimethylhept -3-en-2-yl)-7a-methyloctahydro-4H-inden-4-one (3S,6R,E)-6-((1R,3aS,7aR,E)-4-(2-((3R,5R)-3,5-bis ((tert-butyldimethylsilyl)oxy)cyclohexylidene) ethylidene)-7a-methyloctahydro-1H-inden-1-yl)- 2,3-dimethylhept-4-en-2-ol 2-((3R,5R)-3,5-bis(tert-butyldiMethylsilyloxy)cyclohexylidene)ethanol