Welcome to chemicalbook!
Chinese English Japanese Germany Korea
010-86108875
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 2-TERT-BUTYLIMINO-2-DIETHYLAMINO-1,3-DIMETHYL-PERHYDRO-1,3,2-DIAZAPHOSPHORINE
98015-45-3

2-TERT-BUTYLIMINO-2-DIETHYLAMINO-1,3-DIMETHYL-PERHYDRO-1,3,2-DIAZAPHOSPHORINE synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 2.) 50percent aq. KOH / acetonitrile / 1.) 50 deg C, 24 h
2: 2a) tBuOCl, 50percent KOH; 2b) 75percent aq. HPF6 / 1) 100 deg C, 7 h; 2a) r.t., 3 h

References:

Schwesinger, Reinhard;Willaredt, Juergen;Schlemper, Helmut;Keller, Manfred;Schmitt, Dieter;Fritz, Hans [Chemische Berichte,1994,vol. 127,# 12,p. 2435 - 2454]