9H-9-Silafluorene synthesis
- Product Name:9H-9-Silafluorene
- CAS Number:244-96-2
- Molecular formula:C12H10Si
- Molecular Weight:182.29
Yield:244-96-2 83%
Reaction Conditions:
Stage #1: n-butyllithium;2,2'-dibromobiphenyl in tetrahydrofuran;hexane at -78 - 20; for 2 h;Inert atmosphere;Schlenk technique;
Stage #2: with Dichlorosilane in tetrahydrofuran at -78; for 2 h;Inert atmosphere;Schlenk technique;
References:
Kanno, Ken-ichiro;Hirose, Satoshi;Kyushin, Soichiro [Heteroatom Chemistry,2018,vol. 29,# 5-6,art. no. E21478]
13029-09-9
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244-96-2
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