Acryloylurea synthesis

2synthesis methods

Product Name:Acryloylurea
CAS Number:20602-79-3
Molecular formula:C4H6N2O2
Molecular Weight:114.1

5544-35-4 Synthesis

5544-35-4
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20602-79-3
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Yield:20602-79-3 4.8 g (75%)

Steps:

5 EXAMPLE 5

EXAMPLE 5 In the same manner as in Example 4, the reaction of 7.9 g (20 mmols) of the 3-chloropropionylurea from Example 2 with 7.12 ml (52 mmols) of triethylamine gives the acryloylurea of the formula STR12 Yield: 4.8 g (75%). Melting point: 155-157°C (with decomposition).

References:

US3977881,1976,A

2-Propenoic acid, anhydride with carbamimidic acid, hydrochloride (1:1)

20602-81-7
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20602-79-3
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References

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