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ChemicalBook CAS DataBase List AEEA-AEEA
1143516-05-5

AEEA-AEEA synthesis

1synthesis methods
17-Amino-10-oxo-3,6,12,15-tetraoxa-9-azaheptadecanoic Acid is synthesized by Hydrolysis Reaction of 12,12-Dimethyl-10-oxo-3,6,11-trioxa-9-azatridecanoic acid  with Hydrolysis Reaction in Dichloromethane for 2h.
-

Yield:-

Reaction Conditions:

with trifluoroacetic acid in dichloromethane at 4 - 20;

References:

Clave, Guillaume;Volland, Herve;Flaender, Melanie;Gasparutto, Didier;Romieu, Anthony;Renard, Pierre-Yves [Organic and Biomolecular Chemistry,2010,vol. 8,# 19,p. 4329 - 4345] Location in patent:supporting information; experimental part

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