ChemicalBook CAS DataBase List ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME

ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME synthesis

3synthesis methods

Product Name:ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME
CAS Number:70427-91-7
Molecular formula:C13H24O11
Molecular Weight:356.32

65530-26-9 Synthesis

Methyl4,6-O-benzylidene-a-D-mannopyranoside

65530-26-9
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$68.09/5MG

70427-91-7
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 85 percent / sodium hydride / dimethylformamide / 20 h / 0 deg C to R_.T_.
2: 76 percent / sodium cyanoborohydride, 3A molecular sieves / tetrahydrofuran / 0.5 h / 0 °C
3: mercuric bromide, mercuric cyanide, 4A molecular sieves / acetonitrile / Ambient temperature; 6h then overnight
4: M sodium methoxide / methanol / 2 h / Ambient temperature
5: 91 percent / hydrogen / 10percent palladium-on-charcoal / aq. ethanol; acetic acid / 2625.2 Torr

References:

Madiyalakan, Ragupathy;Chowdhary, Manjit S.;Rana, Surjit S.;Matta, Khushi L. [Carbohydrate Research,1986,vol. 152,p. 183 - 194]

Methyl-4,6-di-O-benzylidene-2,3-di-O-benzyl-α-D-mannopyranoside

51842-18-3
13 suppliers
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70427-91-7
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References

3,4,6-Tri-O-benzyl-beta-D-mannopyranose-1,2-(methyl orthoacetate)

16697-49-7
52 suppliers
$31.00/100mg

70427-91-7
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References

ALPHA-D-MAN-[1->4]-ALPHA-D-MAN-1->OME Related Search:

METHYL ALPHA-L-RHAMNOPYRANOSIDE METHYL-ALPHA-D-MANNOPYRANOSIDE ALPHA-D-MAN-[1->2]-ALPHA-D-MAN-1->OME Methyl 3-O-(α-D-Mannopyranosyl)-α-D-Mannopyranoside