ChemicalBook CAS DataBase List AMINO-(3,4,5-TRIMETHOXY-PHENYL)-ACETIC ACID

AMINO-(3,4,5-TRIMETHOXY-PHENYL)-ACETIC ACID synthesis

4synthesis methods

Product Name:AMINO-(3,4,5-TRIMETHOXY-PHENYL)-ACETIC ACID
CAS Number:86053-97-6
Molecular formula:C11H15NO5
Molecular Weight:241.24

86-81-7 Synthesis

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AMINO-(3,4,5-TRIMETHOXY-PHENYL)-ACETIC ACID

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Yield:-

Steps:

Multi-step reaction with 4 steps
1: Na₂S₂O₅ / methanol; H₂O / 2 h / 35 °C
2: 84 percent / aq. H₂O₂; K₂CO₃ / dimethylsulfoxide / 16.5 h / 21 - 35 °C
3: 92 percent / NaOH; H₂O / various solvent(s) / 3.5 h / Heating
4: hydrazine hydrate; NaOH / Pd/C / H₂O; various solvent(s) / 10 h / Heating

References:

Davies, Antony J.;Ashwood, Michael S.;Cottrell, Ian F. [Synthetic Communications,2000,vol. 30,# 6,p. 1095 - 1102]

Benzeneacetic acid, 3,4,5-trimethoxy-α-[(phenylmethyl)amino]-

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86053-97-6
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References

Benzeneacetonitrile, 3,4,5-trimethoxy-α-[(phenylmethyl)amino]-

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86053-97-6
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References

86053-93-2 Synthesis

Benzeneacetonitrile, α-amino-3,4,5-trimethoxy-

86053-93-2
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86053-97-6
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References