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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List Anagliptin hydrochloride
1359670-56-6

Anagliptin hydrochloride synthesis

4synthesis methods
(S)-tert-butyl 2-(2-(2-cyanopyrrolidin-1-yl)-2-oxoethylaMino)-2-MethylpropylcarbaMate

739365-95-8
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Anagliptin hydrochloride

1359670-56-6
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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: hydrogenchloride / 1,4-dioxane; dichloromethane / 1 h / 20 °C / Cooling with ice
2.1: triethylamine / tetrahydrofuran / 20 °C / Cooling with ice
2.2: 0.17 h / 10 °C

References:

Kato, Noriyasu;Oka, Mitsuru;Murase, Takayo;Yoshida, Masahiro;Sakairi, Masao;Yamashita, Satoko;Yasuda, Yoshika;Yoshikawa, Aya;Hayashi, Yuuji;Makino, Mitsuhiro;Takeda, Motohiro;Mirensha, Yakufu;Kakigami, Takuji [Bioorganic and Medicinal Chemistry,2011,vol. 19,# 23,p. 7221 - 7227]

739364-95-5 Synthesis
2-Methylpyrazolo[1,5-a]pyriMidine-6-carboxylic acid

739364-95-5
240 suppliers
$7.00/250mg

Anagliptin hydrochloride

1359670-56-6
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References
338953-49-4 Synthesis
2-methylpyrazolo[1,5-a]pyrimidine-6-carboxylic acid amide

338953-49-4
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Anagliptin hydrochloride

1359670-56-6
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References
207557-35-5 Synthesis
(2S)-1-(Chloroacetyl)-2-pyrrolidinecarbonitrile

207557-35-5
456 suppliers
$5.00/250mg

Anagliptin hydrochloride

1359670-56-6
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References

Anagliptin hydrochloride Related Search:

1-(2-CHLOROACETYL)PYRROLIDINE-2-CARBOXYLIC ACID Carbamic acid, (2-amino-1,1-dimethylethyl)-, 1,1-dimethylethyl ester (9CI) 2-Pyrrolidinecarbonitrile, 1-(chloroacetyl)- (9CI)