anhalinine synthesis
- Product Name:anhalinine
- CAS Number:642-30-8
- Molecular formula:C12H17NO3
- Molecular Weight:223.27
![Benzenemethanamine, 2,3,4-trimethoxy-N-[2-(phenylthio)ethyl]-](/CAS/20210305/GIF/221128-78-5.gif)
221128-78-5
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642-30-8
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: 98 percent / Ac2O / 1 h / 70 °C
2: 97 percent / NaIO4 / H2O; methanol / 16 h / Ambient temperature
3: 99 percent / TFAA, BF3*OEt2 / benzene / 1 h / Ambient temperature
4: 76 percent / NaBH4, NiCl2*6H2O / methanol; tetrahydrofuran / 0.5 h / Ambient temperature
5: 86 percent / 10 percent NaOH / H2O; ethanol / 1.5 h / Heating
References:
Shinohara, Tatsumi;Takeda, Akira;Toda, Jun;Kohno, Michiyo;Sano, Takehiro [Heterocycles,1999,vol. 51,# 1,p. 119 - 129]
221128-88-7
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642-30-8
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![Formamide, N-[2-(phenylthio)ethyl]-N-[(2,3,4-trimethoxyphenyl)methyl]-](/CAS/20210305/GIF/221128-80-9.gif)
221128-80-9
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642-30-8
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221128-86-5
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642-30-8
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![Formamide, N-[2-(phenylsulfinyl)ethyl]-N-[(2,3,4-trimethoxyphenyl)methyl]-](/CAS/20210305/GIF/221128-82-1.gif)
221128-82-1
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642-30-8
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