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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List AZADO
57625-08-8

AZADO synthesis

7synthesis methods
7-methylidenebicyclo[3.3.1]nonan-3-one

17933-29-8
61 suppliers
$45.00/10mg

AZADO

57625-08-8
35 suppliers
$50.00/5 mg

-

Yield:-

Steps:

Multi-step reaction with 9 steps
1.1: 54 percent / OsO4; NaIO4 / tetrahydrofuran; H2O / 5 h / 20 °C
2.1: 94 percent / p-TsOH*H2O / toluene / 2 h / Heating
3.1: 100 percent / HCl*NH2OH / pyridine / 4 h / 40 °C
4.1: MoO3; NaBH4 / methanol
4.2: 75 percent / Et3N / methanol / 1 h / 0 °C
5.1: 100 percent / aq. HCl / methanol / 2 h / 20 °C
6.1: H2 / Pd/C / methanol / 2 h / 20 °C
7.1: SOCl2 / 1 h / Heating
8.1: LiAlH4 / 1,2-dimethoxy-ethane / 1 h / Heating
9.1: Na2WO4*2H2O / methanol / 0.5 h / 20 °C
9.2: 42 mg / urea hdyrpgenperoxide / methanol / 3.5 h / 20 °C

References:

Shibuya, Masatoshi;Tomizawa, Masaki;Suzuki, Iwao;Iwabuchi, Yoshiharu [Journal of the American Chemical Society,2006,vol. 128,# 26,p. 8412 - 8413]

768-41-2 Synthesis
2-azaadamantane

768-41-2
15 suppliers
inquiry

AZADO

57625-08-8
35 suppliers
$50.00/5 mg

References
5001-18-3 Synthesis
1,3-Adamantanediol

5001-18-3
344 suppliers
$6.00/1g

AZADO

57625-08-8
35 suppliers
$50.00/5 mg

References
BICYCLO[3.3.1]NONANE-3,7-DIONE

770-15-0
37 suppliers
$51.60/100mg

AZADO

57625-08-8
35 suppliers
$50.00/5 mg

References
Spiro[bicyclo[3.3.1]nonane-3,2'-[1,3]dioxolan]-7-one

66077-97-2
0 suppliers
inquiry

AZADO

57625-08-8
35 suppliers
$50.00/5 mg

References