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ChemicalBook CAS DataBase List Batefenterol

Batefenterol synthesis

5synthesis methods
171722-92-2 Synthesis
piperidin-4-yl [1,1'-biphenyl]-2-ylcarbamate

171722-92-2
103 suppliers
$52.00/250mg

-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: tetrahydrofuran; methanol / 16 h / 60 °C
2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / -20 °C
2.2: 6 h
3.1: dichloromethane; methanol / 2 h / 25 °C
3.2: 24 h / 25 °C
4.1: triethylamine hydrofluoride / dichloromethane / 48 h / 25 °C
4.2: 2 h

References:

Shanghai Fengxianqu Center Hospital;Sun Zhenliang;Lv Zhiliang;Wang Heng CN106632257, 2019, B