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ChemicalBook CAS DataBase List BENFURACARB
82560-54-1

BENFURACARB synthesis

1synthesis methods
Benfuracarb is synthesised through a three-step chemical process involving key reagents and controlled reaction conditions. The first step uses triethylamine and disulphur dichloride in chloroform at around 5 DegC for 2.5 hours to initiate the formation of the thioether linkage. The second step involves chlorination in chloroform which helps introduce reactive intermediates. Finally, a second treatment with triethylamine in chloroform for 4 hours at similar temperatures completes the synthesis, yielding benfuracarb.
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: triethylamine; disulfur dichloride / chloroform / 2.5 h / 5 °C
2: chlorine / chloroform / 3 h / 5 - 20 °C
3: triethylamine / chloroform / 4 h / 5 - 20 °C

References:

Hunanhaili Changde Pesticide Chemical Co., Ltd.;Lan Shilin;Liu Weidong;Du Shenghua;Wang Yanli;Liu Yuan;Cheng Chao;Ma Baode CN106674169, 2017, A

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