Benzenamine, 2,4-bis(1-methylethyl)- synthesis
- Product Name:Benzenamine, 2,4-bis(1-methylethyl)-
- CAS Number:79069-41-3
- Molecular formula:C12H19N
- Molecular Weight:177.29
99-62-7
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Yield:79069-41-3 50%
Reaction Conditions:
Stage #1: 1,3-diisopropylbenzenewith pyridine;trifluorormethanesulfonic acid;tetrabutylammonium tetrafluoroborate in acetonitrile at 22;Electrochemical reaction;
Stage #2: with piperidine in acetonitrile at 80; for 12 h;
References:
Herold, Sebastian;M?hle, Sabine;Zirbes, Michael;Richter, Frank;Nefzger, Hartmut;Waldvogel, Siegfried R. [European Journal of Organic Chemistry,2016,vol. 2016,# 7,p. 1274 - 1278] Location in patent:supporting information
33696-11-6
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79069-41-3
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