Benzene, 1-bromo-2-ethenyl-4-(trifluoromethyl)- synthesis
- Product Name:Benzene, 1-bromo-2-ethenyl-4-(trifluoromethyl)-
- CAS Number:1263772-10-6
- Molecular formula:C9H6BrF3
- Molecular Weight:251.04
402-43-7
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere
1.2: 1.08 h / -78 - 20 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / Inert atmosphere; Cooling with ice
2.2: Wittig Olefination / 1 h / 20 °C / Inert atmosphere
References:
Van Hoveln, Ryan;Hudson, Brandi M.;Wedler, Henry B.;Bates, Desiree M.;Le Gros, Gabriel;Tantillo, Dean J.;Schomaker, Jennifer M. [Journal of the American Chemical Society,2015,vol. 137,# 16,p. 5346 - 5354]
1779-49-3
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102684-91-3
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2065-66-9
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$5.00/5g
102684-91-3
185 suppliers
$7.00/1g
1263772-10-6
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